Chemical Analysis of Hydroxyapatite Artificial Bone Powders by Energy Dispersive X-Ray Fluorescence Spectrometry (EDXRF)

Koksal O. K., Apaydin G., Cengiz E., Samek L., Karahan I. H., Tozar A., ...Daha Fazla

SPECTROSCOPY AND SPECTRAL ANALYSIS, cilt.38, sa.8, ss.2645-2649, 2018 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 38 Sayı: 8
  • Basım Tarihi: 2018
  • Doi Numarası: 10.3964/j.issn.1000-0593(2018)08-2645-05
  • Dergi Adı: SPECTROSCOPY AND SPECTRAL ANALYSIS
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.2645-2649
  • Anahtar Kelimeler: EDXRF, X-ray Tube, Elemental analysis, Hydroxyapatite, COATINGS
  • Karadeniz Teknik Üniversitesi Adresli: Evet

Özet

Stoichiometric hydroxyapatite (HA) nanoparticles were synthesized by a wet chemical method. Calcium nitrate tetra hydrate used as calcium source and dibasic ammonium phosphate used as phosphorous source. Calcium nitrate tetra hydrate and dibasic ammonium phosphate solutions were prepared by dissolving the salts in distilled water. Stoichiometric hydroxyapatite nanoparticles used by artificial bone powders and synthesized by a wet chemical method were analyzed using EDXRF method. The concentrations of K, Ca, Ti, V, Cr, Fe, Ni, Cu, Sr and Pb for artificial bone powders have been determined. Besides, Calcium contents were evaluated according to the agitation time and temperature in the production process.