Synthesis and characterization of new metal-free and metallophthalocyanines containing macrocyclic moieties

KANTEKİN H., CELENK E., KARADENIZ H.

JOURNAL OF ORGANOMETALLIC CHEMISTRY, cilt.693, sa.7, ss.1353-1358, 2008 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 693 Sayı: 7
  • Basım Tarihi: 2008
  • Doi Numarası: 10.1016/j.jorganchem.2008.01.037
  • Dergi Adı: JOURNAL OF ORGANOMETALLIC CHEMISTRY
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.1353-1358
  • Karadeniz Teknik Üniversitesi Adresli: Evet

Özet

The synthesis and characterization of new metal-free 7 and metallophthalocyanines 8, 9 carrying macrocyclic N2S2O4 donor groups on peripheral positions have been investigated. Phthalonitrile derivative 6 was synthesized according to Rosenmund von Braun procedure from compound 5. The novel compounds were characterized by elemental analysis, IR, H-1 and C-13 NMR, UV-Vis and MS spectra data. (C) 2008 Elsevier B.V. All rights reserved.