Effects of bleaching agents on the surface microhardness and surface morphology of calcium silicate-based cements: An in vitro study


Naiboğlu P., Koşar T., Yücel A. Ç.

Turkish Endodontic Journal, vol.10, no.3, pp.195-202, 2025 (Scopus)

  • Publication Type: Article / Article
  • Volume: 10 Issue: 3
  • Publication Date: 2025
  • Doi Number: 10.14744/tej.2025.49379
  • Journal Name: Turkish Endodontic Journal
  • Journal Indexes: Scopus
  • Page Numbers: pp.195-202
  • Keywords: Bleaching agents, calcium silicate-based cements, microhardness, surface morphology
  • Karadeniz Technical University Affiliated: Yes

Abstract

Purpose: To assess the effects of exposure to sodium perborate, carbamide peroxide, and hydrogen peroxide on the surface microhardness and surface morphology of ProRoot MTA and Biodentine. Methods: A total of 50 specimens of each cement, ProRoot MTA and Biodentine, were prepared. The specimens were assigned into 5 groups based on the bleaching agent applied (n=10): A mixture of sodium perborate and distilled water (SP-DW), a mixture of sodium perborate and 3% hydrogen peroxide (SP-HP), carbamide peroxide (CP), hydrogen peroxide (HP), and control group. Bleaching agents were changed four times on every fourth day. Surface microhardness and surface morphology were assessed using a microhardness tester and scanning electron microscope, respectively. Data were analysed using two-way ANOVA and Tukey’s test. Results: All bleaching agents caused morphological differences on the surfaces of the both cements. All bleaching agents, except SP-DW, caused a decrease in the microhardness of both cements, with HP causing the greatest decrease, followed by CP and SP-HP, respectively. Biodentine showed higher surface microhardness values than ProRoot MTA in all groups. Conclusion: Biodentine may be recommended as a cervical barrier and a mixture of sodium perborate and distilled water may be the safest bleaching agent to preserve the surface properties of CSCs.