Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques

Nas A., Demirbaş Ü., Gümrükçüoğlu N., Kantekin H.

TURKISH JOURNAL OF CHEMISTRY, cilt.43, sa.1, ss.229-238, 2019 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 43 Sayı: 1
  • Basım Tarihi: 2019
  • Doi Numarası: 10.3906/kim-1807-54
  • Dergi Adı: TURKISH JOURNAL OF CHEMISTRY
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, TR DİZİN (ULAKBİM)
  • Sayfa Sayıları: ss.229-238
  • Karadeniz Teknik Üniversitesi Adresli: Evet

Özet

The complexes of peripherally tetra-substituted metal-free (8), lead(II) (9), and zinc(II) (10) phthalocyanine derivatives were synthesized for the first time in this work. The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, H-1 NMR, C-13 NMR, elemental analysis, and mass spectra. The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.