Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques

Nas A., Demirbaş Ü., Gümrükçüoğlu N., Kantekin H.

TURKISH JOURNAL OF CHEMISTRY, vol.43, no.1, pp.229-238, 2019 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 43 Issue: 1
  • Publication Date: 2019
  • Doi Number: 10.3906/kim-1807-54
  • Journal Name: TURKISH JOURNAL OF CHEMISTRY
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus, TR DİZİN (ULAKBİM)
  • Page Numbers: pp.229-238
  • Karadeniz Technical University Affiliated: Yes

Abstract

The complexes of peripherally tetra-substituted metal-free (8), lead(II) (9), and zinc(II) (10) phthalocyanine derivatives were synthesized for the first time in this work. The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, H-1 NMR, C-13 NMR, elemental analysis, and mass spectra. The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.