QUANTITATIVE-DETERMINATION OF TRIETHANOLAMINE IN CEMENTS

YILMAZ V. T., MENEK N., ODABASOGLU M.

CEMENT AND CONCRETE RESEARCH, cilt.23, sa.3, ss.603-608, 1993 (SCI-Expanded) identifier identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 23 Sayı: 3
  • Basım Tarihi: 1993
  • Doi Numarası: 10.1016/0008-8846(93)90011-w
  • Dergi Adı: CEMENT AND CONCRETE RESEARCH
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.603-608
  • Karadeniz Teknik Üniversitesi Adresli: Hayır

Özet

A new analysis method for the quantitative determination of triethanolamine (TEA) in the aqueous phase of cements was developed. TEA was converted into the TEA-Fe3+ complex by treating it with 1M NaOH and 10% Fe3+ solutions. This method was based on the determination of the TEA-Fe3+ complex by polarographic techniques. The TEA content in the aqueous phase of the tricalcium aluminate-gypsum system was analysed using the analysis method and the amount of TEA adsorbed was found to be approximately 1.5mg per g of the solid phase.