Structure–Property–Radiation Shielding Relationships in Functionally Graded AA2024/B4C Metal Matrix Composites


Karabacak A. H., Çanakçı A., Tunç S. A., Başkan T., Yılmaz A. H.

CRYSTALS, cilt.16, sa.4, ss.274-303, 2026 (SCI-Expanded, Scopus)

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 16 Sayı: 4
  • Basım Tarihi: 2026
  • Doi Numarası: 10.3390/cryst16040274
  • Dergi Adı: CRYSTALS
  • Derginin Tarandığı İndeksler: Scopus, Science Citation Index Expanded (SCI-EXPANDED), Chemical Abstracts Core, Compendex, INSPEC, Directory of Open Access Journals
  • Sayfa Sayıları: ss.274-303
  • Karadeniz Teknik Üniversitesi Adresli: Evet

Özet

Functionally graded AA2024/B4C metal matrix composites were fabricated via mechanical alloying and hot pressing to investigate structure–property–radiation shielding relationships. Single-layer, two-layer, and three-layer architectures with varying B4C contents were systematically produced. Microstructural homogeneity and phase constitution were examined using SEM/EDS and XRD, while thermal stability was evaluated by thermogravimetric analysis. Density and porosity measurements were conducted to assess the influence of reinforcement distribution and functional grading on densification behavior. Gamma radiation shielding performance was experimentally evaluated using a 152Eu source and an HPGe detector over a wide photon energy range. Key shielding parameters, including linear and mass attenuation coefficients, half-value layer, tenth-value layer, mean free path, and radiation protection efficiency, were determined. The results reveal that functional grading significantly enhances radiation attenuation compared to monolithic composites. The three-layer AA2024/B4C composite exhibited the highest attenuation coefficients and the lowest HVL, TVL, and MFP values at all investigated energies, achieving nearly 100% improvement in shielding efficiency relative to unreinforced AA2024. These findings demonstrate that controlled B4C distribution and layered composite architecture provide a synergistic improvement in thermal stability, physical integrity, and radiation shielding performance, positioning functionally graded AA2024/B4C composites as efficient lightweight materials for advanced radiation shielding applications. These results indicate that the developed functionally graded AA2024/B4C composites are promising candidates for advanced radiation shielding applications in nuclear facilities, aerospace structures, and medical radiation protection systems, where lightweight and high-performance materials are critically required.