The synthesis, using microwave irradiation and characterization of novel, metal-free and metallophthalocyanines

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ACAR İ., KANTEKİN H., BIYIKLIOĞLU Z.

JOURNAL OF ORGANOMETALLIC CHEMISTRY, cilt.695, sa.2, ss.151-155, 2010 (SCI-Expanded, Scopus)

• Yayın Türü: Makale / Tam Makale
• Cilt numarası: 695 Sayı: 2
• Basım Tarihi: 2010
• Doi Numarası: 10.1016/j.jorganchem.2009.10.021
• Dergi Adı: JOURNAL OF ORGANOMETALLIC CHEMISTRY
• Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
• Sayfa Sayıları: ss.151-155
• Anahtar Kelimeler: Microwave, Phthalocyanine, Cyclotetramerization, Phthalonitrile, Nickel, Cobalt, ASSISTED SYNTHESIS, PHTHALOCYANINES
• Karadeniz Teknik Üniversitesi Adresli: Evet

Özet

The synthesis of novel metal-free (4) and metallophthalocyanines (5, 6, 7 and 8) were prepared by cyclotetramerization of a novel 4-[2-(1-naphthyloxy)ethoxy]phthalonitrile (3). New substitute phthalocyanines showed the enhanced solubility in organic solvents. The new compounds were characterized by a combination of IR, H-1 NMR, C-13 NMR, UV-Vis and MS spectral data. (C) 2009 Elsevier B. V. All rights reserved.