Sonochemical syntheses and characterization of a new nano-sized 2-D lead(II) coordination polymer as precursor for preparation of PbBr(OH) nano-structure

Sadeghzadeh, Homa; Morsali, Ali; YILMAZ, VEYSEL; Buyukgungor, Orhan

doi:10.1080/00958972.2010.511202

Sonochemical syntheses and characterization of a new nano-sized 2-D lead(II) coordination polymer as precursor for preparation of PbBr(OH) nano-structure

Sadeghzadeh H., Morsali A., YILMAZ V. T., Buyukgungor O.

JOURNAL OF COORDINATION CHEMISTRY, cilt.63, sa.19, ss.3423-3430, 2010 (SCI-Expanded, Scopus)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 63 Sayı: 19
Basım Tarihi: 2010
Doi Numarası: 10.1080/00958972.2010.511202
Dergi Adı: JOURNAL OF COORDINATION CHEMISTRY
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.3423-3430
Anahtar Kelimeler: Nano-structure, Coordination polymer, Lead(II), Crystal structure, RAY-POWDER DIFFRACTION, BISMUTH OXIDE, HYDROTHERMAL PROCESS, CRYSTAL-STRUCTURE, NANOSTRUCTURES, MICROCRYSTALS, COMPLEXES, GROWTH
Karadeniz Teknik Üniversitesi Adresli: Hayır

Özet

Nano-particles of a new 2-D Pb(II) coordination polymer, [Pb(4-pyc)(Br)(H2O)]n (1) (4-Hpyc = 4-pyridinecarboxylic acid), were synthesized by a sonochemical method. Crystal structure of 1 was determined by X-ray crystallography. The nano-particles were characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy, and elemental analyses. PbBr(OH) nano-structure was obtained by the calcination of nano-particles of 1 at 400 degrees C.